13440-07-8, Di(naphthalen-1-yl)phosphine oxide is a chiral-phosphine-ligands compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Add 2-methoxyphenylacetylene (0.066 g, 0.5 mmol) to the reaction flask.Dinaphthylphosphorus (0.30 g, 1 mmol),CuCl (0.01 g, 0.1 mmol), di-tert-butyl peroxide(0.45 g, 3 mmol),And N-methylpyrrolidone (2 mL),70oC reaction;TLC tracks the reaction until it is completely over;The crude product obtained after the reaction is separated by column chromatography(Ethyl acetate: petroleum ether = 1:1) gave the desired product (yield: 73%)., 13440-07-8
The synthetic route of 13440-07-8 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Nantong Textile Silk Industrial Technology Institute; Soochow University (Suzhou); Zou Jianping; Tao Zekun; Lv Shuaishuai; Li Chengkun; Li Jianan; (12 pag.)CN109096336; (2018); A;,
Phosphine ligand
Chiral phosphine ligands in asymmetric synthesis. Molecular structure and absolute configuration of (1,5-cyclooctadiene)-(2S,3S)-2,3-bis(diphenylphosphino)butanerhodium(I) perchlorate tetrahydrofuran solvate