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Reaction of the precursor complexes [Fe2(mu-SCH2Ph)2(CO)6] 1 and [Fe2(mu-SEt)2(CO)6] A with the phosphine ligand (L=P(PhOMe-p)3) yielded the mono-substituted complexes [Fe2(mu-SCH2Ph)2(CO)5(P(PhOMe-p)3)] 2 and [Fe2(mu-SEt)2(CO)5(P(PhOMe-p)3)] 3. All the complexes were characterized by various spectroscopic techniques. X-ray crystal structure has been reported for complex 3. The reduction potentials of the phosphine substituted complexes 2 and 3 appeared at more negative potentials in comparison to the precursor complexes 1 and A. Complexes 1?3 were catalytically active towards proton reduction in the presence of acids.
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Phosphine ligand,
Chiral phosphine ligands in asymmetric synthesis. Molecular structure and absolute configuration of (1,5-cyclooctadiene)-(2S,3S)-2,3-bis(diphenylphosphino)butanerhodium(I) perchlorate tetrahydrofuran solvate