Downstream synthetic route of 13689-19-5

The synthetic route of 13689-19-5 has been constantly updated, and we look forward to future research findings.

13689-19-5, Tricyclohexylphosphine oxide is a chiral-phosphine-ligands compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated

A mixture of 296.4 mg of tricyclohexylphosphorus oxide and 188.5 mg of DyCl3 ¡¤6H2O was added to a beaker, 15 mL of ethanol and 5 mL of water were added, and the mixture was stirred at room temperature for 4 hours. Then, the mixed solution was allowed to stand at room temperature for 3 days to obtain colorless rectangular crystals. The resulting crystals were washed with iced ethanol to purify the resulting product. The calculated yield based on the metal Dy was 52%.

The synthetic route of 13689-19-5 has been constantly updated, and we look forward to future research findings.

Reference£º
Patent; Nankai University; Cheng Peng; Wang Yuxia; Shi Wei; (8 pag.)CN107556341; (2018); A;,
Phosphine ligand
Chiral phosphine ligands in asymmetric synthesis. Molecular structure and absolute configuration of (1,5-cyclooctadiene)-(2S,3S)-2,3-bis(diphenylphosphino)butanerhodium(I) perchlorate tetrahydrofuran solvate