An update on the compound challenge: 14694-95-2

The article 《Homogeneous rhodium ion catalyst encapsulated by benzoyl-terminated dendrimer: high hydrogenation and separation capabilities for diene copolymers》 also mentions many details about this compound(14694-95-2)Electric Literature of C54H45ClP3Rh, you can pay attention to it, because details determine success or failure

Most of the natural products isolated at present are heterocyclic compounds, so heterocyclic compounds occupy an important position in the research of organic chemistry. A compound: 14694-95-2, is researched, SMILESS is [Rh]Cl.P(C1=CC=CC=C1)(C2=CC=CC=C2)C3=CC=CC=C3.P(C4=CC=CC=C4)(C5=CC=CC=C5)C6=CC=CC=C6.P(C7=CC=CC=C7)(C8=CC=CC=C8)C9=CC=CC=C9, Molecular C54H45ClP3RhJournal, Colloid and Polymer Science called Homogeneous rhodium ion catalyst encapsulated by benzoyl-terminated dendrimer: high hydrogenation and separation capabilities for diene copolymers, Author is Zhou, Wei; Qu, Wenwen; Peng, Xiaohong, the main research direction is rhodium catalyst encapsulated benzoyl terminated dendrimer hydrogenation nitrile rubber; SBR nitrile rubber hydrogenation catalyst dendrimer.Electric Literature of C54H45ClP3Rh.

Benzoyl chloride was employed to react with primary amino groups on the surface of the second generation of poly(propylene imine) (G2-PPI) dendrimer to synthesize benzoyl-terminated dendrimer (G2-B) by a nucleophilic substitution reaction. A novel homogeneous catalyst of G2-B(Rh3+) was prepared by complexing RhCl3·3H2O with G2-B, and further applied to the catalytic hydrogenation of nitrile rubber (NBR) and styrene-butadiene rubber (SBR). The hydrogenation degrees (HDs) of HNBR and HSBR catalyzed by G2-B(Rh3+) are 99.2 and 92.1% resp. The contents of Rh residue in the HNBR and HSBR catalyzed by G2-B(Rh3+) are only 41 and 31 ppm, resp., which are resp. decreased by 84.5 wt% and 83.2 wt%, resp., compared to those catalyzed by RhCl(PPh3)3.

The article 《Homogeneous rhodium ion catalyst encapsulated by benzoyl-terminated dendrimer: high hydrogenation and separation capabilities for diene copolymers》 also mentions many details about this compound(14694-95-2)Electric Literature of C54H45ClP3Rh, you can pay attention to it, because details determine success or failure

Reference:
Phosphine ligand,
Chiral phosphine ligands in asymmetric synthesis. Molecular structure and absolute configuration of (1,5-cyclooctadiene)-(2S,3S)-2,3-bis(diphenylphosphino)butanerhodium(I) perchlorate tetrahydrofuran solvate