Synthetic Route of 1038-95-5, An article , which mentions 1038-95-5, molecular formula is C21H21P. The compound – Tri-p-tolylphosphine played an important role in people’s production and life.
Reaction of [AuCl(SMe2)] with para-ethynylaniline and para-ethynyl-ortho-toluidine affords oligomers, [Au(CC-4-C6H 3RNH2)]n (R = H, Me), which in turn react with tertiary phosphines or 2,5-dimethylphenylisocyanide to give monomeric adducts, [Au(C?C-4-C6H3RNH2)L]. One of these, [Au(CC-4-C6H4NH2){P(3-tolyl)3}], has been crystallographically characterised and is a polymer in the solid state, being held together via NH?Au contacts.
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Reference：
Phosphine ligand,
Chiral phosphine ligands in asymmetric synthesis. Molecular structure and absolute configuration of (1,5-cyclooctadiene)-(2S,3S)-2,3-bis(diphenylphosphino)butanerhodium(I) perchlorate tetrahydrofuran solvate