Synthetic Route of 166330-10-5. Chemistry is an experimental science, and the best way to enjoy it and learn about it is performing experiments.Introducing a new discovery about 166330-10-5, Name is (Oxybis(2,1-phenylene))bis(diphenylphosphine)
Designing of Ferromagnetic 3D Hierarchical Core-Shell Fe3O4@NiO/Co3O4 Microspheres Derived from a MOF Precursor: As an Efficient Catalyst for C-P Cross Coupling Reaction
Herein, we report the synthesis of a 3D hierarchical heterostructure microsphere through a facile solvothermal and hydrothermal method followed by an annealing treatment. The obtained ternary core-shell nanostructured was comprehensively characterized by means of variety techniques including FT-IR, XRD, BET, TEM, FE-SEM, EDX, EDX-mapping, VSM and ICP-OES. It was found that this hierarchical nanostructured could promote the C?P cross coupling reaction of a large library of functional substrates. Benefiting from the unique hierarchical architecture and the synergistic effect among multiple components resulted from the coexistence of micro-, meso- and macropores as well as its small nano-crystallite size (20-71 nm), this novel catalyst revealed superior catalytic performance in the C?P cross coupling reaction. More importantly, the ferromagnetic behavior of 3D hierarchical core-shell Fe3O4@NiO/Co3O4 microspheres is responsible for easy separation from the reaction mixture using an external magnetic field and its long term-durability under reaction conditions even after nine consecutive recycle runs.
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Reference£º
Phosphine ligand,
Chiral phosphine ligands in asymmetric synthesis. Molecular structure and absolute configuration of (1,5-cyclooctadiene)-(2S,3S)-2,3-bis(diphenylphosphino)butanerhodium(I) perchlorate tetrahydrofuran solvate