13440-07-8, Di(naphthalen-1-yl)phosphine oxide is a chiral-phosphine-ligands compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
General procedure: Into a round bottom flask was added p-(difluoroiodo)toluene (1, 0.17 mmol, 1.1 equiv) and PhCl (0.25 mL, 0.6M), followed by the secondary phosphine oxide (3, 0.15 mmol, 1.0 equiv). The resulting reaction mixture was stirred at 60 C in a pre-heated oil bath for 10 minutes, by which time TLC analysis indicated consumption of the starting material. The crude reaction mixture was cooled to room temperature and directly purified by column chromatography (ether/pentane) without prior concentration., 13440-07-8
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Reference£º
Article; Eljo, Jasmin; Murphy, Graham K.; Tetrahedron Letters; vol. 59; 31; (2018); p. 2965 – 2969;,
Phosphine ligand
Chiral phosphine ligands in asymmetric synthesis. Molecular structure and absolute configuration of (1,5-cyclooctadiene)-(2S,3S)-2,3-bis(diphenylphosphino)butanerhodium(I) perchlorate tetrahydrofuran solvate