13440-07-8, Di(naphthalen-1-yl)phosphine oxide is a chiral-phosphine-ligands compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Add 4-trifluoromethylphenylacetylene to the reaction flask(0.085 g, 0.5 mmol), dinaphthylphosphoric acid(0.30 g, 1 mmol), CuI2 (0.032 g, 0.1 mmol),Phenylisopropyl hydroperoxide (0.46 g, 3 mmol),And N,N-dimethylformamide (2 mL),70oC reaction;TLC tracks the reaction until it is completely over;The crude product obtained after the completion of the reaction was separated by column chromatography (ethyl acetate: petroleum ether = 1:1) to give the desired product.(Yield 82%)., 13440-07-8
The synthetic route of 13440-07-8 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Nantong Textile Silk Industrial Technology Institute; Soochow University (Suzhou); Zou Jianping; Tao Zekun; Lv Shuaishuai; Li Chengkun; Li Jianan; (12 pag.)CN109096336; (2018); A;,
Phosphine ligand
Chiral phosphine ligands in asymmetric synthesis. Molecular structure and absolute configuration of (1,5-cyclooctadiene)-(2S,3S)-2,3-bis(diphenylphosphino)butanerhodium(I) perchlorate tetrahydrofuran solvate