With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.24171-89-9,Tri(thiophen-2-yl)phosphine,as a common compound, the synthetic route is as follows.
A hexane solution (30 mL) of 4 (20 mg, 0.23 mmol) and PTh3 (10 mg, 0.035 mmol) was heated to reflux for 1 h during, during which time the color of the solution changed from pale yellow to orange. The solvent was then removed under reduced pressure and the residue was subjected to TLC on silica gel. Elution with hexane/CH2Cl2 (7:3, v/v) developed only one band that corresponded to 5 (16 mg, 61%)., 24171-89-9
The synthetic route of 24171-89-9 has been constantly updated, and we look forward to future research findings.
Reference£º
Article; Uddin, Md Miaz; Begum, Noorjahan; Ghosh, Shishir; Sarker, Jagodish C.; Tocher, Derek A.; Hogarth, Graeme; Richmond, Michael G.; Nordlander, Ebbe; Kabir, Shariff E.; Journal of Organometallic Chemistry; vol. 812; (2016); p. 197 – 206;,
Phosphine ligand
Chiral phosphine ligands in asymmetric synthesis. Molecular structure and absolute configuration of (1,5-cyclooctadiene)-(2S,3S)-2,3-bis(diphenylphosphino)butanerhodium(I) perchlorate tetrahydrofuran solvate