With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.13689-20-8,Cyclohexyldiphenylphosphine oxide,as a common compound, the synthetic route is as follows.
Add cyclohexyldiphenylphosphine oxide (28.4 mg, 0.1 mmol) to the reaction flask.Copper triflate (3.6 mg, 0.01 mmol), tetramethyldisilazane (26.7 mg, 0.2 mmol) and toluene (1 mL), and the mixture was stirred at 80 C;TLC tracks the reaction until it is completely over;The crude product obtained after the completion of the reaction was recrystallized from toluene to give the desired product (yield: 82%)., 13689-20-8
As the paragraph descriping shows that 13689-20-8 is playing an increasingly important role.
Reference£º
Patent; Soochow University (Suzhou); Zou Jianping; Li Chengkun; Tao Zekun; (13 pag.)CN110229187; (2019); A;,
Phosphine ligand
Chiral phosphine ligands in asymmetric synthesis. Molecular structure and absolute configuration of (1,5-cyclooctadiene)-(2S,3S)-2,3-bis(diphenylphosphino)butanerhodium(I) perchlorate tetrahydrofuran solvate