With the rapid development and complex challenges of chemical substances, new drug synthesis pathways are usually the most effective.63995-70-0,Sodium 3,3′,3”-phosphinetriyltribenzenesulfonate,as a common compound, the synthetic route is as follows.,63995-70-0
Under argon protection,Add to 50mLSchlenk bottle1 ¡¤ 56 mmol of (SO3Na+) 3-R6,4 ¡¤ 73 mmol of [CH3 (EO) 42N + H = C (N (CH3) 2) 2] [CH3SO3-] and 25 mL of acetonitrile,The reaction mixture was stirred at room temperature for 72 hours, filtered,The filtrate was removed under reduced pressure to give an orange yellow viscous liquid acetonitrile, yield 96%.
The synthetic route of 63995-70-0 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Qingdao University of Science and Technology; JIN, XIN; LI, SHU MEI; ZHAO, KUN; (11 pag.)CN103483381; (2016); B;,
Phosphine ligand
Chiral phosphine ligands in asymmetric synthesis. Molecular structure and absolute configuration of (1,5-cyclooctadiene)-(2S,3S)-2,3-bis(diphenylphosphino)butanerhodium(I) perchlorate tetrahydrofuran solvate