1608-26-0, N,N,N’,N’,N”,N”-Hexamethylphosphinetriamine is a chiral-phosphine-ligands compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Compound 6 (526.211 eq) was added to the Schlenk tube,After evacuation of nitrogen,The system was cooled to 0 C,And the reaction vessel was added at this temperatureP (NMe2) 3 (1.3 eq),Reaction at 0 C for 10 min,Then rose to 110 C,TLC detection to complete reaction,Separation by column chromatography to give a white solid,The yield was 80%
The synthetic route of 1608-26-0 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Shangqiu Teachers College; Zhengzhou University; Zhao, Wenxian; Chao, Ruiqing; Li, Gaowei; Xu, Kai; Wang, Tao; Wang, Xiaojuan; Zhao, Ruijuan; Liu, Lantao; (16 pag.)CN104530122; (2016); B;,
Phosphine ligand
Chiral phosphine ligands in asymmetric synthesis. Molecular structure and absolute configuration of (1,5-cyclooctadiene)-(2S,3S)-2,3-bis(diphenylphosphino)butanerhodium(I) perchlorate tetrahydrofuran solvate